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“救心丹”为由日本进口的主治心脏不适的成药。其包装标示处方含麝香、牛黄、蟾酥、熊胆、犀角、人参、真珠、龙脑,含药量甚低。用常规显色反应检验,专属性不强,取样量太大。本文用薄层层析法于硅胶-G板上选用6种展开溶剂系统,取样品6粒,以按其处方自行配制的对照品及各药材的提取液作参比对照,检验麝香、龙脑、牛黄、熊胆、蟾酥、人参。10批样品均能检出麝香、龙脑、牛黄、蟾酥、人参,同时其中9批检不出熊胆的特征成分——熊去氧胆酸,而检出猪去氧胆酸。作为定性方法,本法取样量少,较准确简便,易于推广。
“Sai Xin Dan” is a medicine for indwelling heart disease imported from Japan. Its package label prescription contains musk, bezoar, osmanthus, bear bile, rhino horn, ginseng, pearl, borneol, and the drug content is very low. With the conventional color reaction test, the specificity is not strong, and the sampling volume is too large. In this paper, six kinds of developing solvent systems were selected on a silica gel-G plate by thin-layer chromatography, six samples were taken, and the control products prepared according to the prescription and extracts of each medicinal material were used as reference controls to test the musk and borneol. , Niuhuang, bear gall, glutinous rice cake, ginseng. Ten batches of samples were able to detect musk, borneol, bezoar, osmanthus, and ginseng. At the same time, 9 batches of ursodeoxycholic acid, a characteristic component of bear bile, could not be detected. Hyodeoxycholic acid was detected. As a qualitative method, this method has a small sample size, is more accurate, simpler, and easier to promote.