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在碱性催化下,用酸酐或酰卤使环硫雄醇发生酯化反应,合成了环硫雄醇-17β-乙酸酯和新 化合物环硫雄醇-17β-对氯苯甲酸酯。反应在2-3小时内完成,收率较高。
Under alkaline catalysis, cyclic thioxanthenol was esterified with acid anhydride or acid halide to synthesize cyclic thiostanol-17β-acetate and new compound cyclic thiostanol-17β-p-chlorobenzoate. The reaction is completed in 2-3 hours, the yield is higher.