Synthesis, Crystal Structure and Biological Activity of a Novel Amino Acid Salt (HGly)_4[HPMo_(12)

• 出 处: Chemical Research in Chinese Universities
• 发表日期: 2003年01期
• 关键词: coordinated interact carboxylate HGly HPMo H_2O Synthesis glycine distorted dres

A novel compound, (HGly) 4[HPMo 12 O 40 ] 2·22H 2O, was synthesized and characterized by means of elemental analysis, IR and X ray diffraction. The compound crystallized in a monoclinic space group Cc with a =4 0060(0 8) nm, b =1 2527(0 3) nm, c =1 9930(0 4) nm, β =96 36(3)°, V =9 940(3) nm 3, Z =2, R 1=0 0576, wR 2 =0 1746. The anti tumor activity of this compound was tested in two human tumor cell lines in vitro .

A novel compound, (HGly) 4 [HPMo 12 O 40] 2 · 22H 2O, was synthesized and characterized by means of elemental analysis, IR and X-ray diffraction. The compound crystallized in a monoclinic space group Cc with a = 4 0060 ( 0 8) nm, b = 1 2527 (0 3) nm, c = 1 9930 0 4 nm, β = 96 36 3 °, V 9 940 3 nm 3, Z 2, R 1 = 0 0576, wR 2 = 0 1746. The anti tumor activity of this compound was tested in two human tumor cell lines in vitro.