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本文叙述了氯苯在人体内残留量的检测。脂肪组织取自南斯拉夫斯洛文尼亚共和国两家医院1979~1980年死于车祸、年龄20~60岁的男女遇难者。人乳汁取自1981年9~10月间在卢布尔雅那市产科诊所分娩后3~5天的母乳。样本冰冻保存备测。脂肪组织分析样本重1g,用10 ml正己烷溶解,加入20ml浓硫酸振摇。然后用10ml浓硫酸清洗两次已烷提取液。让已烷提取液通过
This article describes the detection of residual chlorobenzene in the human body. Fat tissue was obtained from men and women aged 20 to 60 who died in a car accident in two hospitals in the Republic of Slovenia in Yugoslavia from 1979 to 1980. Human milk is obtained from breast milk from 3 to 5 days after giving birth at the obstetric clinic in Ljubljana between September and October 1981. Frozen samples prepared for testing. Aliquots of adipose tissue samples were weighed 1 g, dissolved in 10 ml of n-hexane, and shaken with 20 ml of concentrated sulfuric acid. The hexane extract was then washed twice with 10 ml of concentrated sulfuric acid. Let hexane extract through