INDUCTION PLASMA REACTIVE DEPOSITION OF TUNGSTEN CARBIDE FROM TUNGSTEN METAL POWDER

来源 :Acta Metallurgica Sinica(English Edition) | 被引量 : 0次 | 上传用户:iqplll
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Experimental results are reported on the primary carburization reaction between the tungsten powder and methane in the induction plasma, and the secondary carburiza tion of the deposit on substrate at high temperature. Optical microscopy and scanning electron microscopy were used to examine the microstructures of starting tungsten powder, carburized powder, and deposit. X-ray diffraction analysis, thermal gravimet ric analysis and microhardness measurement were used to characterize the structures and properties of the powder and the deposit. It is found that the primary carbur ization reaction in the induction plasma starts from the surface of tungsten particles when the particles are melted. Tungsten particles are partially carburized inside the reactive plasma. Complete carburization is achieved through the secondary carburiza tion reaction of the deposit on substrate at high temperature. Experimental results are reported on the primary carburization reaction between the tungsten powder and methane in the induction plasma, and the secondary carburiza tion of the deposit on substrate at high temperature. Optical microscopy and scanning electron microscopy were used to examine the microstructures of the starting tungsten powder , carburized powder, and deposit. X-ray diffraction analysis, thermal gravimet ric analysis and microhardness measurement were used to characterize the structures and properties of the powder and the deposit. It is found that the primary carburization reaction in the induction plasma starts from the surface of tungsten particles when the particles are melted. Tungsten particles are partially carburized inside the reactive plasma. Complete carburization is achieved through the secondary carburization reaction of the deposit on substrate at high temperature.
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