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A family of aluminum powder filled epoxy-phenolic resins were prepared and characterized over a broad range of phenolic/epoxy/aluminum weight ratios.The effect of the filler on the thermal properties of the cured resin was studied by using TGA and the results show that the thermal stability of filled polymer is significantly greater than that of unfilled one.These aluminum filled epoxy-phenolic resins were coated on a glass fabric carrier to form a tape adhesive.