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以碘活化的六乙基亚磷酰三胺为磷酰化及环化试剂，经一锅法合成并分离得到硫代环磷酸酯的两个非对映异构体，并对这两个非对映异构体的性质进行了研究．
Iodine-activated hexaethylphosphoric triamide is a phosphorylation and cyclization reagent. Two diastereoisomers of thiocyclophosphates are synthesized and separated by one-pot method. The enantiomeric properties were studied.