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本文报导了间甲酚与二甲二硫醚进行甲硫基化反应的规律。采用“高酚量低温反应”和“有机溶剂萃取后处理工艺”使标题化合物合成收率达85—90%,纯度达95%左右。
This article reports the law of methylthiolation of m-cresol and dimethyl disulfide. The high yield of phenol and low temperature reaction and the organic solvent extraction and post-treatment process make the yield of the title compound 85-90% and the purity about 95%.