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目的:建立心舒丸的质量标准。方法:采用气相色谱法测定冰片中龙脑的含量;采用高效液相色谱法测定丹参中丹酚酸B的含量。结果:龙脑在0.100 3～5.015 0μg范围内呈良好线性关系,平均回收率99.1%,RSD=1.2%(n=6);丹酚酸B在0.090 8～1.816μg范围内线性关系良好,平均回收率97.5%,RSD=1.4%(n=6)。结论:该方法重复性、准确性良好,可作为标准用于心舒丸质量的控制。
Objective: To establish the quality standard of Xinshuwan. Methods: The content of borneol in borneol was determined by gas chromatography. The content of salvianolic acid B in salvia miltiorrhiza was determined by high performance liquid chromatography. Results: The range of 0.100 3 ~ 5.015 0μg ranged from 0.2g to 0.42g. The average recovery rate was 99.1%, RSD was 1.2% (n = 6). The linear range of salvianolic acid B in the range of 0.090 8 ~ 1.816μg was good. The mean Recovery was 97.5%, RSD = 1.4% (n = 6). Conclusion: The method is reproducible and accurate, which can be used as a standard for the quality control of XSH.