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<Abstract>Two novel triazolyl derivatives with biphenyl links, namely 4,4-bis(1,2,4-triazol-1-yl-methyl)biphenylene 1 and 4,4-bis(3,5-dimethyl-1,2,4-triazol-1-ylmethyl)biphenylene 2, have been synthesized and structurally characterized by single-cry