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Radiation-induced defect annealing in He~+ ion-implanted 4 H-SiC via H~+ ion irradiation is investigated by Raman spectroscopy. There are 4 H-SiC wafers irradiated with 230 keV He~+ ions with fluences ranging from 5.0×10~(15) cm~(-2)to 2.0×10~(16) cm~(-2) at room temperature. The post-implantation samples are irradiated by 260 keV H~+ ions at a fluence of 5.0×10~(15) cm~(-2) at room temperature. The intensities of Raman lines decrease after He implantation,while they increase after H irradiation. The experimental results present that the magnitude of Raman line increment is related to the concentration of pre-existing defects formed by He implantation. A strong new peak located near 966 cm~(-1), which is assigned to 3 C-SiC LO(Γ) phonon, is found in the He-implanted sample with a fluence of 5.0×10~(15) cm~(-2) followed by H irradiation. However, for the He-implanted sample with a fluence of2.0×10~(16) cm~(-2) followed by H irradiation, no 3 C-SiC phonon vibrations are found. The detailed reason for H irradiation-induced phase transformation in the He-implanted 4 H-SiC is discussed.
Radiation-induced defect annealing in He ~ + ion-implanted 4 H-SiC via H ~ + ion irradiation is investigated by Raman spectroscopy. There are 4 H-SiC wafers irradiated with 230 keV He ~ + ions with fluences ranging from 5.0 × 10 ~ (15) cm ~ (-2) to 2.0 × 10 ~ (16) cm ~ (-2) at room temperature. The post-implantation samples were irradiated by 260 keV H ~ + ions at a fluence of 5.0 × 10 ~ (15) cm -2 at room temperature. The intensities of Raman lines decrease after He implantation, while they increase after H irradiation. The experimental results present that the magnitude of Raman line increment is related to the concentration of pre-existing A strong new peak located near 966 cm -1, which is assigned to 3 C-SiC LO (Γ) phonon, is found in the He-implanted sample with a fluence of 5.0 × 10 ~ (15) cm ~ (-2) followed by H irradiation. However, for the He-implanted sample with a fluence of 2.0 × 10 ~ (16) cm -2 followed by H irradiation, no 3 C-SiC phonon vibrations are found Detailed reason for H irradiation-induced phase transformation in the He-implanted 4 H-SiC is discussed.