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由(NH4)2WS4、AgI和Bu4NBr用低热温固相反应合成了类立方烷簇合物[Bu4N]3·[WAg3S4I4]。用X射线单晶衍射法测定其晶体结构。
The quasi-cubic paraffin cluster [Bu4N] 3 · [WAg3S4I4] was synthesized from (NH4) 2WS4, AgI and Bu4NBr by low temperature solid-state reaction. The crystal structure was determined by single crystal X-ray diffraction.