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目的建立舒心通络丸的质量标准。方法采用TLC法鉴别方中黄芪、丹参、川芎、红花和远志;采用HPLC法测定陈皮中橙皮苷的含量。结果黄芪、丹参、川芎、红花和远志TLC色谱斑点清晰,专属性好;橙皮苷在0.3255μg~2.1700μg范围内线性关系良好(r=0.9999),平均加样回收率为98.86,RSD=1.37%。结论该薄层色谱鉴别方法斑点清晰、专属性强、重现性好,含量测定方法分离度好、结果准确,可有效控制舒心通络丸的质量。
Objective To establish the quality standard of Shuxintongluo Pills. Methods Radix Astragali, Radix Salviae Miltiorrhizae, Rhizoma Chuanxiong, safflower and Polygala tenuifolia were identified by TLC, and the content of hesperidin in dried tangerine peel was determined by HPLC. Results The chromatograms of Astragalus membranaceus, Radix Salviae Miltiorrhizae, Rhizoma Chuanxiong, safflower and Polygalae were clear and specific. Hesperidin had a good linearity (r = 0.9999) in the range of 0.3255μg ~ 2.1700μg with an average recovery of 98.86, RSD = 1.37%. Conclusion The method of TLC identification is characterized by clear spots, strong specificity, good reproducibility, good separation of content determination methods and accurate results, which can effectively control the quality of Shuxintongluo pill.