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Systematical experiments were done at five temperature levels: (500 ℃,) (630 ℃,) (900 ℃,) (1 000 ℃) and (1 100 ℃) to illuminate the layer structure of the multi-layered metal-intermetallic composites of Ni-Al system that were fabricated by a previously reported simple and cost-effective method. The analysis of back scattering photos and XRD examination of specimens reveal that the look like single compound layer is composed of several different components. The primary phase produced during reaction is Ni_2Al_3 and there exists a like two-phase field between NiAl_3 and Ni_2Al_3. The high temperature phases like NiAl and Ni_3Al are also found at low temperature. The results indicate that the key driving force of in-situ reaction is not temperature, but the atom concentration.
Systematical experiments were done at five temperature levels: (630 ° C, 900 ° C, 1000 ° C) and (1 100 ° C) to illuminate the layer structure of the multi-layered metal-intermetallic composites of The analysis of back scattering photos and XRD examination of specimens reveal that the look like single compound layer is composed of several different components. The primary phase produced during reaction is Ni_2Al_3 and there exists a like two-phase field between NiAl_3 and Ni_2Al_3. The high temperature phases like NiAl and Ni_3Al are also found at low temperature. The results said that the key driving force of in-situ reaction is not temperature, but the atom concentration.