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Fe/Ti multilayers with different modulation wavelengths (A) prepared by r.f. sputtering has been investigated by using cross sectional transmission electron microscopy (XTEM). It was observed that the columnar structure, interface morphology, and metastable phase presented at the interface of the multilayer system strongly depend on the bilayer thickness (A) For high period multilayers, the waviness wavelength of interfaces is about two times broader than the column diameter. For a sample with A=30 nm, its column width and waviness wavelength was about 80, and 190 nm, respectively. Both of them decreased with the reduction of A, so as to nearly equal values of column diameter and waviness wavelength were obtained. The Fe and Ti grains of both 30 nm and 6 nm multilayers are polycrystalline, and have a textured structure. In short bilayer thickness (A=6 nm), the intermetallic compound Fe2Ti was presented at the interfaces due to solid state reaction; for A=2 nm, amorphous phase Ti-rich layer was formed at the interfaces, resulting in a sharp interface multilayer structure.
It was observed that the columnar structure, interface morphology, and metastable phase presented at the interface of the multilayer (A) prepared by rf sputtering has been investigated by using cross-sectional transmission electron microscopy (XTEM) system strongly depend on the bilayer thickness (A) For high period multilayers, the waviness wavelength of interfaces is about two times broader than the column diameter. For a sample with A = 30 nm, its column width and waviness wavelength was about 80, and Both of them decreased with the reduction of A, so as to nearly equal values of column diameter and waviness wavelength were. The Fe and Ti grains of both 30 nm and 6 nm multilayers are polycrystalline, and have a textured In short bilayer thickness (A = 6 nm), the intermetallic compound Fe2Ti was presented at the interfaces due to solid state reaction; for A = 2 nm, amorphous phase Ti-rich l ayer was formed at the interfaces, resulting in a sharp interface multilayer structure.