CRYSTAL AND MOLECULAR STRUCTURE OF 1,2, 3-TRIBENZOYLINDOLIZINE

• 出 处: 结构化学
• 发表日期: 1993年01期
• 关键词: conjugated yellow benzoyl instead verify melting Lorentz petroleum deter remaini

Crystal and molecujar structure of the title compound, C29H19NO3, was determined by single crystal X-ray diffraction analysis. .Mt=429. 48, monoclin-ic, space group P21/n, a = 10. 365 (3), b= 14. 614(4), c= 14. 857 (4) A ,β= 103.55(2)°,V=2186. 1(10) A3, Z=4, Dc= 1. 30g/cm3,μ(MoKa) = 0. 81cm-1, F (000) = 919. 87. Final residual R value was 0. 0704 and Rw = 0. 0704. The indo-hzine ring is conjugated only with the 1-benzonyl group.

Crystal and molecular structure of the title compound, C29H19NO3, was determined by single crystal X-ray diffraction analysis. Mt = 429. 48, monoclin- ic, space group P21 / n, a = 10. 365 (3), b = 14. 614 (4), c = 14. 857 (4) A, β = 103.55 (2) °, V = 2186.1 A3, Z = 4, Dc = 1.30 g / cm3, μ ) = 0.81 cm-1, F (000) = 919. 87. Final residual R value was 0. 0704 and Rw = 0. 0704. The indo-hzine ring was conjugated only with the 1-benzonyl group.