Synthesis,Crystal Structure and Thermal Analysis of N-（2,3-Dimethyl-phenyl）-N＇-（methoxyl formyl）thio

• 作 者: ZHAO Dan HUANG Jie SONG Ji-ron
• 机 构: ShaanxiKeyLaboratoryofPhysico-inorganicChemistry,ConservationTechnologyDepartment
• 出 处: 高等学校化学研究：英文版
• 发表日期: 2012年2期
• 关键词: 甲基苯基 晶体结构 甲酰基 甲氧基 合成 硫脲 热分析 标题化合物 X-Ray diffraction Acylthiourea Crystal structu
• 基金项目: Supported by the National Natural Science Foundation of China（No.20571060）, the Natural Science Foundation of Shaanxi Province China（No.2007B08）

N-(2,3-Dimethyl-phenyl)-N'-(methoxyl formyl)thiourea was synthesized by the reacting of 2,3-dimethylaniline,potassium thiocyanate(KSCN) and methyl chloroformate(ClCOOCH 3).Single crystal was obtained by slowly evaporation solvent at room temperature.T