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应用IR、MS和EPR表征CuCl和NH4Y固态离子交换过程以及制备Cu（Ⅰ）Y的一些特性.固态离子交换程度依赖于反应温度.和还原Cu（Ⅱ）Y得到Cu（Ⅰ）Y的方法，固态离子交换是更为有效的制备纯Cu（Ⅰ）Y的方法．
The solid state ion exchange process of CuCl and NH4Y and some properties of Cu (Ⅰ) Y were characterized by IR, MS and EPR. The degree of solid state ion exchange depends on the reaction temperature and the method of reducing Cu (Ⅱ) Y to obtain Cu (Ⅰ) Y. Solid state ion exchange is a more effective method for preparing pure Cu (I) Y.