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采用同位素稀释法和相对灵敏度因子法定量分析了99.999~99.9999%Tm_2O_3中20多种稀土及非稀土杂质含量,测定下限0.0X~0.00Xμg/g,大多数元素相对标准偏差在30%以内,同位素稀释法所测Zn、Ba、Eu的相对标准偏差在10%。
The isotopic dilution method and relative sensitivity factor method were used to quantitatively analyze the contents of more than 20 rare earth and non-rare earth impurities in 99.999-99.9999% Tm 2 O 3. The lower limit of determination was 0.0X ~ 0.00Xμg / g, the relative standard deviation of most elements Within 30%, the relative standard deviation of Zn, Ba and Eu measured by isotope dilution method is 10%.