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In this study, MoS2/reduced graphene oxide hybrid material (MoS2/RGO) was synthesized through a facile and effective hydrothermal method.Fe-Ni matrix composites with different weight fractions of MoS2/RGO were prepared by powder metallurgy (P/M) technique (1%, 3%, 5%, 7%), and their tribological properties at the temperature ranging from room temperature to 600 ℃ were investigated using a UMT-2 ball-on-plate friction and wear tester.