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In this paper,Bituminous coal,coconut shell and hawkthom stone were used as raw materials to produce activated carbons (ACs).Iodine adsorption,N2 adsorption [1],pH value,Boehm titration [2],TPR [3] were used to characterize the pore structure and surface chemical properties of ACs; FTIR was used to evaluate the variation of functional groups after TPR.