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To maintain a high dispersion and high stability of active metals are still a tough issue for heterogeneous catalysts due to easy aggregation or leaching.Herein, we demonstrated a preparation of colloidal nanocatalysts Pd@CBFS (polybenzoxazine-based carbon nanospheres) by impregnating H2PdCl4 solution on polymer at room temperature, followed by a thermal treatment under N2 atmosphere.