Copper-catalyzed Synthesis of gem-Difluoromethylene moiety Linked Diheterocyclic Compounds

来源 :中国化学会第十六届全国有机合成化学学术研讨会 | 被引量 : 0次 | 上传用户:study_sky
下载到本地 , 更方便阅读
声明 : 本文档内容版权归属内容提供方 , 如果您对本文有版权争议 , 可与客服联系进行内容授权或下架
论文部分内容阅读
  Heterocycles such as 2-oxindoles and benzo-1,3-diazoles have become the privileged scaffolds for pharmaceutical design and drug discovery and hold a special place among pharmaceutically significant natural products and synthetic compounds.[1] Furthermore,the often at the C-3 substituted of 2-oxindoles and C-2 position substituted of benzo-1,3-diazoles can effectively enhance the biological activity of these compounds.On the other hand,two pharmacophoric groups covalently bounded via a linkage are expected to elicit increased pharmacological action or dual efficacy.[2] Therefore,it is highly prospective to develop the facile and efficient method for gem-difluoromethylene moiety linked diheterocyclic compounds through benzo-1,3-azolic(oxa-or thia-)difluoromethyl radicals generated by Cu(I)single electron transformation was added to terminal of C-C double bond of N-arylacrylamides,followed by cyclization to 2-oxindoles under mild conditions(Scheme 1).
其他文献
手性共轭分子与聚合物广泛用于有机光电材料和器件,包括光伏电池、有机发光二极管、荧光传感器等,相关的研究工作引起了人们极大的关注.螺烯是一类至少由四个芳(杂)环邻位稠合而成的具有螺旋手性结构的芳香化合物.螺烯在合成化学、材料化学、分子识别以及不对称催化等领域中的广泛潜在用途,因而成为化学和材料学家们最感兴趣的体系之一.目前文献报道的螺烯的制备方法主要是化学合成法,主要包括D-A环化反应、钯催化分子内
A 3D imidazole-bearing cyclophane cage L1 was synthesized as trivalent cationic templates to react with metal halide to obtain a novel organic-inorganic crystalline hybrid: {[CdI4]3·(L1)2}(1).1,2 Its
硫氰酸酯是一类重要的合成原料,也是具有生物活性的结构单元。经典合成硫氰酸酯方法主要有两种:(1)硫氰酸盐与含有特定取代基的有机物反应;(2)硫醇的有机酸酯或二硫醚作为次磺酰基来源与氰基化试剂反应[1]。本课题组发现了一种通过硫醚脱烷基氰基化制备芳基硫氰酸酯的新型方法,氟试剂(Selectfluor)为氧化物,TMSCN为氰基化试剂[2]。该方法操作简单、步骤经济,避免了硫醇恶臭给使用者带来的不便。
有机太阳能电池具有成本低、质量轻、柔韧性好、半透明等独特的优点,并且基于非富勒烯受体材料的单节太阳能电池器件的光电转换效率已经超过了15%,引起广泛关注.梯形双吡喃母核可以有效地拓宽材料的吸收光谱,减少其带隙,同时π桥引入,有利于LUMO能级提升.1氧族五元杂环(呋喃、噻吩和硒吩)多被运用在聚合物侧链以及共轭主链上,对分子的构型、共混膜的形貌、材料的带隙等有一定的调节作用.2本文以梯形双吡喃Ph-
Phenothiazine,a linearly fused nitrogen-and sulfur-containing tricyclic compounds,has been become one of the most important heterocycles due to its valuable chemical properties and significant biologi
The copper-catalyzed asymmetric propargylic substitution reaction offers valuable access to enantioenricheed,terminal-alkyne-containing products[1].This reaction is of significant value because termin
Coumarin is a privileged scaffold that frequently occurred in a large number of natural products,pharmaceuticals and agrochemicals.1 3-quaternary carbon oxindoles constitute the framework of a wide va
会议
会议
Pincer iridium complexes have been widely used as catalysts in organic transformations.In particular,a variety of achiral Ir pincers are found to be very efficient catalysts for(de)hydrogenation and t