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本文以乙二醇和乙醇为溶剂，柠檬酸钠为络合剂，采用溶剂热法用乙二醇同时还原氧化石墨和氯化钯制备了 Pd/石墨烯催化剂，研究了柠檬酸钠加入量对催化剂结构和催化甲酸氧化性能的影响。采用透射电镜(TEM)、X射线衍射(XRD)、循环伏安和计时电流对催化剂进行了表征和性能评价。
一步还原法制备纳米Pd/石墨烯及其对甲酸的电催化氧化
【摘 要】
：
本文以乙二醇和乙醇为溶剂，柠檬酸钠为络合剂，采用溶剂热法用乙二醇同时还原氧化石墨和氯化钯制备了 Pd/石墨烯催化剂，研究了柠檬酸钠加入量对催化剂结构和催化甲酸氧化性能的影响。采用透射电镜(TEM)、X射线衍射(XRD)、循环伏安和计时电流对催化剂进行了表征和性能评价。
【机 构】
：
河南省表界面科学重点实验室,郑州轻工业学院,郑州450002
【出 处】
：
河南省化学会2016年学术年会
【发表日期】
：
2016年10期
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