Synthesis and Crystal Structure of 2-(4-Oxo-3-o- tolyl-3,4-dihydroquinazolin-2-ylthio)acetohydrazide

• 作 者: Aamer Saeed Shams-ul-Mahmood U
• 机 构: DepartmentofChemistry,DepartmentChemie
• 出 处: 结构化学
• 发表日期: 2012年9期
• 关键词: 晶体结构 合成 甲苯基 喹唑啉 单晶X-射线衍射 氧代 二氢 酰肼 quinazolinone acetohydrazide synthesis
• 基金项目: The author gratefully acknowledges a research grant from the HigherEducation Commission of Pakistan under project No. 4-279/PAK-US/HEC 2010-917

The title compound was synthesized from 3-(2-methylphenyl)-2-thioxo-2,3-dihy- droquinazolin-4(1H)-one (4) which was prepared from 2-methylaniline in two steps. The structure was supported by the spectroscopic data and unambiguously confirmed by single-cry