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利用动态力学分析（ＤＭＡ）．透射电子显微镜（ＴＥＭ）和小角Ｘ光光散射（ＳＡＸＳ）对聚砜（ＰＳＦ）、聚二甲基硅氧烷（ＰＤＭＳ）和聚对羟基苯乙烯（ＰＨＳ）三元多嵌段共聚物ＰＳＦ—ＰＤＭＳ—ＰＨＳｎ的形态结构进行了研究．结果表明，ＰＳＦ—ＰＤＭＳ—ＰＨＳｎ的形态结构出现了许多新的现象，除具有微相分离的基本特征外，还出现双连续相双分散相的特征．在适当的嵌段长度和组成下，通过ＴＥＭ观察到一种新的特殊形态蜂窝状形态结构，并在嵌段共聚物两相界面处直接观察到非常清晰的界面相．同时，对该形态的形成过程作了初步讨论．
Using Dynamic Mechanical Analysis (DMA). (PSF), polydimethylsiloxane (PDMS) and poly (p-hydroxystyrene) (PHS) ternary multiblock copolymers were characterized by transmission electron microscopy (TEM) and small angle X-ray light scattering (SAXS) The morphological structure of PSF-PDMS-PHSn was studied. The results show that there are many new phenomena in the morphological structure of PSF-PDMS-PHSn. In addition to the basic characteristics of microphase separation, the characteristics of bicontinuous phase doubly dispersed phase appear. Under the appropriate block length and composition, a new special morphological-honeycomb morphological structure was observed by TEM, and a very clear interface phase was directly observed at the two-phase interface of the block copolymer. At the same time, the forming process of this form has been preliminarily discussed.