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应用气相色谱／质谱（ＧＣ／ＭＳ）法对一例速可眠中毒病人生物样品进行分析鉴定。样品经酸化、乙醚提取，然后于ＧＣ／ＭＳ分析，在患者胃内容物和血中检出速可眠，在眼药３３ｈ尿内可检出速可眠原型药物以及四个代谢产物。并用外标法对生物样品中速可眠进行定量测定，对临床救治起到了积极作用。
A sample of patients with rapid sleep poisoning was analyzed and identified by gas chromatography / mass spectrometry (GC / MS). Samples were acidified, extracted with ether, and then analyzed by GC / MS. The contents of gastric contents and blood in patients were detected as fast as possible. And with the external standard method for biological samples in the quasi-sleep quantitative determination of clinical treatment has played a positive role.