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  5. One-pot synthesis of 2-(1-acyloxypentyl) benzoic acids

One-pot synthesis of 2-(1-acyloxypentyl) benzoic acids

来源 :中国化学快报 | 被引量 : 0次 | 上传用户：lili00789563241
【摘 要】
：
A one-pot synthesis of 2-(1-acyloxypentyl) benzoic acids by trapping the carboxylate/alkoxide dianion with acylating reagents following Grignard addition with n
【作 者】
：
Zhen Li Min Yi Hua Zhang Yi Sh 
【机 构】
：
Center of Drug Discovery
【出 处】
：
中国化学快报
【发表日期】
：
2004年期
【关键词】
：
One-pot synthesis 3-n-Butyl-1(3H)-isobenzofuranone 2-(1-Hydroxypentyl)benzoie ac 
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A one-pot synthesis of 2-(1-acyloxypentyl) benzoic acids by trapping the carboxylate/alkoxide dianion with acylating reagents following Grignard addition with n-BuMgBr to 2-formylbenzoic acid was described. Compared with routine synthetic method, this novel procedure has the advantage of convenient operation and higher yields.
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