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The synthesis of nanosized powders and their assembly is of considerable importance to the microelectronics industry because of the pervasive drive to miniaturize components. In this work, silver (Ag) nanoparticls was syntheized. Polygonal silver nanoparticls were synthesized by reacting AgNO3 with hydroquinone, in the presence of poly-(vinylpyrrolidone) (PVP) and an ionic liquid 1-n-butyl-3-methylimidazolium hexafluoroborate ([BMIM]·PF6) at ambient temperature. XRD shows that the crystal structure of the nanoparticles is face-centered cubic. TEM measurements display the silver particles with uniform size and narrow particle size distributions. The UV-Vis spectra of the nanoplates distinguish from those of the samples prepared in the absence of PVP and/or ILs. This method is facile and the as-prepared silver nanoparticls are also stable in some solvents, such as ethanol and water.