Low Temperature Solvent Evaporation-induced Crystallization Synthesis of Nanocrystalline TiO_2 Photo

来源 :Chinese Journal of Chemistry | 被引量 : 0次 | 上传用户:axyyuan
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A novel and efficient methodology for obtaining highly active photocatalyst of bi phase TiO 2 with small particle size and high specific surface area was developed by solvent evaporation induced crystallization (SEIC) method at low temperature. The prepared TiO 2 powder was characterized with X ray diffraction (XRD), transmission electron microscopy (TEM) and BET surface areas. The photocatalytic activity was evaluated by the photocatalytic oxidation of acetone in air. The results showed that the photocatalytic activity of the TiO 2 powder prepared by this method approached that of Degussa P25. This may be attributed to the fact that the prepared TiO 2 powder had larger specific surface areas (265 m 2·g -1 ) and smaller crystallite size (about 5 nm), but relatively low crystallinity, as compared with Degussa P25. A novel and efficient methodology for obtaining highly active photocatalyst of bi phase TiO 2 with small particle size and high specific surface area was developed by solvent evaporation induced crystallization (SEIC) method at low temperature. The prepared TiO 2 powder was characterized with X-ray diffraction The photocatalytic activity was evaluated by the photocatalytic oxidation of acetone in air. The results showed that the photocatalytic activity of the TiO 2 powder prepared by this method approached that of Degussa P25 . This may be attributed to the fact that the prepared TiO 2 powder had larger specific surface areas (265 m 2 · g -1) and smaller crystallite size (about 5 nm), but relatively low crystallinity, as compared with Degussa P25.
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