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以甲醇-氯仿(3∶1)为提取溶剂,采用双波长薄层扫描法,在苦味酸硅胶G薄层板上,氯仿-醋酸乙酯-甲醇(90∶7∶3)为展开剂,在λS=500nm,λR=600nm下,测定了中药制剂盘根接骨片中血竭素的含量,其结果平均回收率为97.4%,相对标准差为1.8%.
Using chloroform-ethyl acetate-methanol (90: 7: 3) as developing solvent, using a two-wavelength thin layer scanning method on a thin layer of picric acid silica gel with methanol-chloroform λS = 500nm, λR = 600nm, the content of Dracorhodin in Panjin jiegu tablet was determined. The average recovery was 97.4% and the relative standard deviation was 1.8%.