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采用提拉法以固液同成分配比（Ｌｉ２ＣＯ３／Ｎｂ２Ｏ５＝４８．６／５１．４）生长了Ｆｅ掺杂及（Ｚｎ，Ｆｅ）、（Ｍｇ，Ｆｅ）和（Ｃｅ，Ｆｅ）双掺杂ＬｉＮｂＯ３（ＬＮ）单晶。Ｃｅ∶Ｆｅ∶ＬｉＮｂＯ３晶体的质量，指数增益系数和衍射效率皆高于Ｆｅ∶ＬｉＮｂＯ３晶体。所测得（Ｚｎ，Ｆｅ）∶ＬＮ、（Ｃｅ，Ｆｅ）∶ＬＮ、（Ｍｇ，Ｆｅ）∶ＬＮ和Ｆｅ∶ＬｉＮｂＯ３晶体的抗光致散射能力分别为８．２×１０３，３．２×１０２，８．３×１０２和１．２×１０２Ｗ／ｃｍ３；在４８８ｎｍ光进行的光折变实验中还原处理后的（Ｃｅ，Ｆｅ）∶ＬｉＮｂＯ３晶体具有最高的二波耦合增益系数，为４０．２ｃｍ－１，其全息衍射效率可达８２．２％；实验结果表明（Ｚｎ，Ｆｅ）∶ＬｉＮｂＯ３和（Ｍｇ，Ｆｅ）∶ＬｉＮｂＯ３具有抗光散射能力强，响应时间短的特点，而（Ｃｅ，Ｆｅ）∶ＬｉＮｂＯ３的增益系数和衍射效率均为最高，明显优于Ｆｅ∶ＬｉＮｂＯ３晶体。
Czochralski (Fe) and (Zn, Fe), (Mg, Fe) and (Ce, Fe) doping were grown by the Czochralski method with the solid-liquid ratio of Li2CO3 / Nb2O5 = 48.6 / LiNbO3 (LN) single crystal. The mass, exponential gain coefficient and diffraction efficiency of Ce: Fe: LiNbO3 crystal are higher than that of Fe: LiNbO3 crystal. The measured values of (Zn, Fe): LN, (Ce, Fe): LN, (Mg, Fe): LN and Fe: LiNbO3 were 8.2 × 103,3.2 × 102 , 8.3 × 102 and 1.2 × 102W / cm3, respectively. The photoluminescence experiments at 488nm showed that the (Ce, Fe): LiNbO3 crystals had the highest two-wave coupling gain coefficient of 40.2cm The results show that (Zn, Fe): LiNbO3 and (Mg, Fe): LiNbO3 have the characteristics of strong light scattering ability and short response time, while the (Ce, Fe ): The gain coefficient and diffraction efficiency of LiNbO3 are the highest, obviously better than Fe: LiNbO3 crystal.