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概述了在温和条件下,CO催化偶联合成草酸酯,主要研究了原料气的浓度、反应温度等因素对产物的影响,以及钯络合物催化剂的性能.对反应机理也进行了探讨.“,”This paper studied the catalytic coupling synthesis of oxalic ester from CO under mild conditions. The effects of the reaction conditions, such as the concentration of gas and reaction temperature are investigated.The performance of the Pd complex catalyst is also investigated