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选用失水山梨醇单油酸酯／反应物水溶液／环己烷制成微乳液等“微反应器”，在其中控制反应，制备出了具有球形及棒状、不规则片状与球形但呈细胞器状排布的纳米氧化锌。用透射电镜（TEM）、动态激光光微射（DLLS）与X－射线衍射对产物的结构、形态、大小与化学成分进行了表征。系统研究了反应体系的组分、配比、反应温度及分散方法等反应条件对“微反应器”与产物形态、大小的影响。探讨了ZnO纳米粒子的稳定性及其原因。并对ZnO纳米粒子的紫外—可见光吸收性能进行了表征。
The micro-reactor such as sorbitan monooleate / reactant solution / cyclohexane was used as the microemulsion, and the reaction was controlled in the reaction to prepare spherical or rod-shaped, irregular flakes and spherical but organelles Shape arrangement of nano zinc oxide. The structure, morphology, size and chemical composition of the product were characterized by transmission electron microscopy (TEM), dynamic laser light scattering (DLLS) and X-ray diffraction. The effects of reaction conditions, such as the composition of the reaction system, the ratio, the reaction temperature and the dispersion method, on the morphology and size of the “microreactor” and the product were systematically studied. The stability and reasons of ZnO nanoparticles were discussed. The UV-Vis absorption properties of ZnO nanoparticles were characterized.