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The crystal structure of the title compound(C17H12ClFO5,Mr=350.72) was determined by single-crystal X-ray diffraction.The crystal belongs to monoclinic,space group P21/c,with a=7.693(1),b=15.767(1),c=12.986(1),β=97.23(1)°,V=1562.6(2)3,Z=4,Dc= 1.491 g/cm3,λ(MoKα)=0.71073,F(000)=720,μ(MoKα)=0.280 mm-1,R=0.0563 and wR=0.1674.A total of 3592 unique reflections were collected,of which 2462 with Ⅰ>2σ(Ⅰ) were observed.Five-membered lactone rings and hydroxyl-substituted phenyl rings are approximately coplanar with their dihedral angle of 4.1°.The dihedral angle between two different phenyl rings is 71.3°.To our interest,intramolecular O(1)-H(1)···O(4) hydrogen bonds could be found in each molecule.Intramolecular hydrogen bonds and intermolecular van der Waals force contribute to the stability of the structure.
The crystal structure of the title compound (C17H12ClFO5, Mr = 350.72) was determined by single-crystal X-ray diffraction. The crystal belongs to monoclinic space group P21 / c with a = 7.693 (1), b = 15.767 , c = 12.986 (1) β, β = 97.23 (1) °, V = 1562.6 (2) 3, Z = 4, Dc = 1.491 g / cm3, λ (MoKα) = 0.71073, F 720, μ (MoKα) = 0.280 mm-1, R = 0.0563 and wR = 0.1674.A total of 3592 unique reflections were collected, of which 2462 with I> 2σ (I) were observed.Five-membered lactone rings and hydroxyl- substituted phenyl rings are approximately coplanar with their dihedral angle of 4.1 °. The dihedral angle between two different phenyl rings is 71.3 ° .To our interest, intramolecular O (1) -H (1) ··· O (4) hydrogen bonds could be found in each molecule. Intramolecular hydrogen bonds and intermolecular van der Waals force contribute to the stability of the structure.