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The dual-bath coagulation method was used for the preparation of PES membrane in this experiment . The main intent of this study was to assess the efforts of gelation conditions on the structures and properties .The dense top layer as well as porous supporting layer can be made by dnel-bath coagulation method simultaneously. Different internal quench medium obtained different membrane with different structures. With the increase in time in the first coagulation bath, pure water flux decreased and the clearance rates of urea and creatirine both first increased then decreased and increased slightly in the end. With the temperature of the second coagulation bath increasing, pure water flux increases and the clearance rates of urea and creatinine first increases then decreases and increases a little at last. Higher DMSO concentration ( wt/ wt ) in the second coagulation bath results in the increase of pure water flux and the decrease of urea & creatinine clearance rates.