【摘 要】
：
为了扩大喷雾干燥技术在生物物料微粒制备方面的应用,在自行设计的实验台上,以超临界CO2为干燥介质进行了乙基纤维素微粒的制备.研究了喷嘴出口直径、气液比、溶液浓度、温度
【机 构】
：
上海理工大学食品与低温研究所,莱阳农学院食品科学系,复旦大学药学院
论文部分内容阅读
为了扩大喷雾干燥技术在生物物料微粒制备方面的应用,在自行设计的实验台上,以超临界CO2为干燥介质进行了乙基纤维素微粒的制备.研究了喷嘴出口直径、气液比、溶液浓度、温度、压力对微粒粒径及其粒径分布的影响.实验结果表明:改变工艺参数,可在较大范围内调控微粒大小,所制微粒平均粒径为1.07～9.84μm;气液出口为8 mm的喷嘴所得微粒粒径比4 mm的要小且分布变窄、粒度均匀;气液比对微粒粒径的影响存在一个粒径最大值;高浓度溶液所得微粒粒径比低浓度溶液大,粒径分布略有变宽;随温度升高,微粒粒径增大,高温时所得微粒的粒径分布比低温时宽;随压力增加,微粒粒径减小,高压时所得微粒的粒径分布比低压时略有变窄.
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