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采用水热合成法合成了标题化合物C7H7NO2·C10H8N2,并测定了其晶体结构.该晶体属于三斜晶系,P-1空间群,晶体学参数为:a=8.3253(18),b=9.980(2),c=10.099(2);α=116.340(2)°,β=90.435(3)°,γ=90.354(3)°,V=751.9(3)3,Z=2,Dc=1.296 mg/m3,最终偏差因子R1=0.0531,wR2=0.1366(I>2σ(I)).该化合物通过分子间氢键形成一维链状结构.
The title compound C7H7NO2 · C10H8N2 was synthesized by hydrothermal synthesis and its crystal structure was determined. The crystal belongs to the triclinic system P-1 space group with the following crystallographic parameters: a = 8.3253 (18), b = 9.980 ( Α = 116.340 (2) °, β = 90.435 (3) °, γ = 90.354 (3) °, V = 751.9 (3) 3, Z = 2, Dc = 1.296 mg / m3, the final deviation factor R1 = 0.0531, wR2 = 0.1366 (I> 2σ (I)). The compounds formed a one-dimensional chain structure through intermolecular hydrogen bonding.