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一、前言 由于热导式(热流式)量热计可以连续地记录量热池内的热功率曲线,近年来它作为研究反应过程的一种新型仪器广泛地应用到各种领域。但是测量信号相对于池内反应的滞后现象,使得记录曲线不能正确地反映实际过程,在放热速率明显地大于传热速率的情况下则更为严重。如果直接用失真了的热谱图去研究被测过程,必然会带来误差甚至错误。因此,恢复热
I. INTRODUCTION Since the thermal conductivity calorimeter can continuously record the thermal power curve in the calorimeter, it has been widely used in various fields as a new type of instrument for studying the reaction process in recent years. However, the hysteresis of the measured signal relative to the in-cell reaction makes the recording curve not correctly reflect the actual process, which is more serious when the heat release rate is significantly greater than the heat transfer rate. If you directly use the distorted thermogram to study the measured process, it is bound to bring errors or even errors. So, recover heat