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The hydrothermal reaction of 1,2-bis(imidazol-1′-yl)ethane (Bime) and Ni(NO3)2·6H2O gave rise to a two-folded interpenetrating 3D coordination polymer, [Ni(Bime)3·(NO3)2]n. Singlecrystal X-ray diffraction analyses show that the complex crystalli