Synthesis and Crystal Structure of 15,16-Bis（（4-nitrophenoxy）methyl）-2,3,5,6,8,9,11,12- octahydroben

• 作 者: HAN Jian-Rong ZHEN Xiao-Li TIA
• 机 构: CollegeofSciences,CollegeofChemical＆PharmaceuticalEngineering
• 出 处: 结构化学
• 发表日期: 2012年2期
• 关键词: 晶体结构分析 硝基苯 合成 苯并15冠5 无水碳酸钾 标题化合物 分子间氢键 X-射线 double-armed crown ether crystal st
• 基金项目: The project was supported by the Natural Science Foundation of Hebei Province （No. B2009000670） and the Foundation of the Education Department of Hebei Province （No. 2009117）

Double-armed crown ether 15,16-bis((4-nitrophenoxy)methyl)-2,3,5,6,8,9,11,12-octahydrobenzo[b][1,4,7,10,13] pentaoxacyclopentadecine F.W. 570.54 was synthesized by dibromomethyl benzo-15-crown-5 with 4-nitrophenol in the presence of anhydrous K2CO3, chara