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Macrocyclic tri- and tetra-amines containing a hydroxyl group in the ring have been prepared in moderate yields by a 1:1 cyclocondensation of l,3-dichloro-2-propanol with the disodium salt of N-tosylated diethylenetriamine and triethylenetetraamine.In the case of condensation of 1,3-dichloro-2-propanol with the disodium salt of N-tosylated diethylenetriamine,the 2:2 cyclocondensation product,dihydroxyl macrocyclic hexaamine,was also isolated.