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采用套管法(PIT)制备Bi系高温超导带材,进行了冷压工艺的优化研究。试验结果表明,Bi系带材所能承受的压力有一个限值,若超过这个限值后,密度虽可提高,但晶粒破碎严重,JC值反而降低。带材优化的冷压工艺参数是838℃/60h+冷压+838℃/60h+冷压+838℃/60h;第一次压力为2GPa,第二次为2.5GPa;冷压压下速率为1.75×10-4mm/s。同时研究还表明,冷压的主要作用是提高带材的致密度和晶粒取向度,从而最终改善带材的超导性能。
Bi-based high-temperature superconducting tapes were prepared by the casing method (PIT), and the optimization of cold-pressing process was studied. The experimental results show that there is a limit to the pressure that the Bi-based strip can withstand. If the limit is exceeded, the density will increase but the grain will be broken severely and the JC value will decrease. The optimum parameters of cold-rolling process are 838 ℃ / 60h + cold pressing + 838 ℃ / 60h + cold pressing + 838 ℃ / 60h; the first pressure is 2GPa and the second is 2.5GPa; the rate of cold pressing is 1.75 × 10-4mm / s. At the same time, the research also shows that the main effect of cold pressing is to increase the density and grain orientation of the strip, and ultimately improve the superconductivity of the strip.