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本文报导了无水无氧条件下的单晶制备方法，主要有液体扩散法、气体扩散法和降温法．实验表明这些方法具有良好的效果，且可使用于对空气不敏感化合物的单晶制备
This paper reports the preparation of single crystals under anhydrous and anaerobic conditions, mainly including liquid diffusion method, gas diffusion method and cooling method. Experiments show that these methods have good effects and can be used for single crystal preparation of air-insensitive compounds