CRYSTAL STRUCTURE OF MIXED METAL CLUSTER Ni_2Nb_2Te_4 OBTAINED BY SOLID STATE REACTION

来源 :结构化学 | 被引量 : 0次 | 上传用户:lilianmm
下载到本地 , 更方便阅读
声明 : 本文档内容版权归属内容提供方 , 如果您对本文有版权争议 , 可与客服联系进行内容授权或下架
论文部分内容阅读
The compound Ni2Nb2Te4 crystallizes in orthorhombic system,space group Pma2 with cell dimensions a = 7.955(1),b=6.258(1),c=7.202(2)A,and Z=2.X-ray structural determination showed the non-molecular 2-dimensional character of the title compound. In each structural unit, the two Ni and two Nb atoms form a rhombic plane with four Ni-Nb bonds (average 2.675 A) and one Ni-Ni bond (2.536 A) and there exists no Nb-Nb interaction. The distorted tetrahedral coordination of each metal atom is completed by four Te atoms. The average distances are 2.799A for Nb-Te bonds and 2.560A for Ni-Te bonds. The compound Ni2Nb2Te4 crystallizes in orthorhombic system, space group Pma2 with cell dimensions a = 7.955 (1), b = 6.258 (1), c = 7.202 (2) A and Z = molecular 2-dimensional character of the title compound. In each structural unit, the two Ni and two Nb atoms form a rhombic plane with four Ni-Nb bonds (average 2.675 A) and one Ni-Ni bond (2.536 A) and there exists no Nb-Nb interaction. The distorted tetrahedral coordination of each metal atom is completed by four Te atoms. The average distances are 2.799A for Nb-Te bonds and 2.560A for Ni-Te bonds.
其他文献
地下水分布范围很广,它可以看作是地下介质的组成部分。大量实测资料说明,地下流体能够较灵敏地反映岩层的应力应变,因此,利用地下水化学组份变化开展地震预报研究具有较广
会计信息对决策有用,使得会计信息具有帮助投资者和贷款者评估和预测企业未来的现金流动进而作出合理决策的作用,并有助于政府部门宏观调控以及有利于企业加强和改善经营管理
云南松分布广泛,西藏东南部、四川泸定及天全以南,贵州毕节以西,广西百色地区都有分布,以云南分布最广,故有云南松之称。云南松多生长在海拔1000—3500米的高山,喜光,耐干旱耐瘠薄,适应酸性的
在三峡宜昌小峰风景区一带,有一种代代相传、民间广泛应用于各种生产、生活、交易之中,由数码字和计量单位组成的,俗称“肉码字”的文字,它别于包括楚人在内的中原民族所创
本文用共沉淀法制备了含有稀土的中温变换催化剂。在铁-铬系中,只添加CeO_2为助催化剂,代替了K_2O、MgO,CaO……等。得到了活性高、强度大、耐热性好的催化剂。经550℃耐热8
据美国BIOCOMPARE科技新闻网(2010-03-05)报道,澳洲的科学家发现,雄性激素会通过环绕心脏血管新生的方式,来避免可能发生的心脏受损现象。 According to the US BIOCOMPARE
环境污染是当今时代无法根除的顽症,原因何在?简单地说,就在于人们过分追求经济效益而忽略环境社会效益。这种“追求”,一者是发展经济的动力使然,另者则是缘于我们早就抨击过的“
The geometrical configurations of the products in reaction of sulfur and ethylene are optimized by use of UHF method and 3-21G basis sets and the potential ene
Human phenylalanine hydroxylase (PAH) cDNA was applied as a hybridization probe to analyzing the following 8 restriction fragment length polymorphisms (RFLP) i
文章收集了近年来50多篇文献,评述了偶氮类试剂与金属离子生成的配合物在滴汞电极上的极谱行为及分析中的应用情况。展望了分析应用的前景。 In this paper, we collected m