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将 (CF3SO2 ) 2 O加入伯酰胺和 Et3N的 CH2 Cl2 溶液中 ,室温搅拌 10~ 2 5 min,制得相应的腈。 11例收率 84~ 95 %。伯酰胺在非酸性条件下制成腈@周琦奕
The (CF3SO2) 2 O added to the primary amide and Et3N in CH2 Cl2 solution, stirred at room temperature for 10 ~ 25 min, the corresponding nitrile. 11 cases yield 84 ~ 95%. Primary amide made under non-acidic conditions nitrile @ Zhou Qi Yi