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In the present investigation,Ni50Ti25Al25 (at.％) mochanically alloyed powder is deposited on carbon steel substrate.Before the coating process,the substrate is heated to temperature ranging from room temperature to 400 ℃.The microstructure,porosity,microhardness,adhesion strength,and corrosion behavior of the coating are investigated at different substrate temperatures.Results show that coating porosity is lower on high temperature surface.Microhardness and adhesion strength of the deposition layer on the substrate without preheating have lower values than with preheating.The polarization test result shows that corrosion performance of the coating is dependent on micro cracks and porosities and the increasing of substrate temperature can improve the quality of coating and corrosion performance.