Photoinduced electron transfer of [ Ru (bpy)_2 (4, 4'-dcbpy)]~(2+) with electron donors

来源 :Chinese Journal of Chemistry | 被引量 : 0次 | 上传用户:liuw_ei
下载到本地 , 更方便阅读
声明 : 本文档内容版权归属内容提供方 , 如果您对本文有版权争议 , 可与客服联系进行内容授权或下架
论文部分内容阅读
Emission quenching of [Ru(bpy)2(4, 4’-dcbpy)] (PF6)2 (1) by benzenamine,4-[2-[5-[4-[4-dimethylamino]phenyl]-4,5-di-hydro-1-phenyl-1H-pyrazol-3-yl]-ethenyl]-N,N-dimetyl (2) or 1, 5-diphenyl-3-(2-phenothiazine)-2-pyrazoline (3) was observed. Measurements of the emission decay of 1 before and after addition of 2 or 3 by single photon counting technique con-finned the observations. The emission quenching of 1 by 2 or 3 was submitted to Stern-Volmer equation. It was calculated that the quenching rate constants (kq) are 5.5 × 109(mol/L)-1s-1 for 2 and 4.0 × 109(mol/L)-1s-1 for 3, respectively. These results indicated a character of dynamic quenching process. The singlet-state of 2 or 3 was also quenched by 1. The quenching behaviors did not conform to the Stern- Volmer equation and involved both static and dynamic quenching processes. The apparent quenching rate constant (kapp) was calculated to be 3 × 109 (mol/L)-1 for the interaction of excited 2 with 1, and 1.2 × 109 (mol/L)-1 for that of excited 3 wit Emission quenching of [Ru (bpy) 2 (4,4’-dcbpy)] (PF6) 2 (1) by benzenamine, 4- [2- [5- [4- [dimethylamino] -di-hydro-1-phenyl-1H-pyrazol-3-yl] -ethenyl] -N, N-dimetyl (2) Measurements of the emission decay of 1 before and after addition of 2 or 3 by single photon counting technique con-finned the observations. The emission quenching of 1 by 2 or 3 was submitted to Stern-Volmer equation. It was calculated that the quenching rate constants (kq) are 5.5 × 109 (mol / L) -1s-1 for 2 and 4.0 × 109 (mol / L) -1s-1 for 3, respectively. These results indicate that a character of the dynamic quenching process The singlet-state of 2 or 3 was also quenched by 1. The quenching behaviors did not conform to the Stern-Volmer equation and involved both static and dynamic quenching processes. The apparent quenching rates constant (kapp) was calculated to be 3 × 109 (mol / L) -1 for the interaction of excited 2 with 1, and 1.2 × 109 (mol / L) -1 for tha t of excited 3 wit
其他文献
目的 探讨OUR—XGD旋转式伽玛刀治疗胶质瘤的疗效。方法 采用OUR—XGD旋转式伽玛刀对 17例胶质瘤和 8例手术残留肿瘤实施治疗。结果 随访 2 1例 ,随访率 84% ,肿瘤消失 6
1病例报告 患者男性,75岁。继往双上肺陈旧性结核及冠心病史。主诉胸前区疼痛半年,服用硝酸甘油不能缓解,进行性加重4个月,不咳嗽,无痰中带血。体格检查:于患者右前胸壁可见
小儿急性汞蒸气中毒二例訾慧芬,李佩铂,殷玉仙(包头市第二医院)例1:女、1.5岁,因咳嗽伴呼吸困难2天入院。入院前两天家长曾在家中土法炼金,有汞蒸气吸入,入院后查:T:36.7℃,呼吸110次/分,精神萎靡昏睡伏
A new Lycopodium alkaloid together with a phenolic glyco-side-arbutin, were isolated from the whole plant of Huperzia serrata. The new compound was assigned th
电影改编是一种艺术的再创造,既要忠实于原著,又要有自己新的理解,但无论怎样改编,都必须符合原著的精神。许鞍华导演较为准确的把握住了原著的神韵,虽然在叙事视角、场景的
入夏以来,山东日照市消防志愿者服务支队改变以往宣传服务形式,选择在市民乘凉较为集中的公园和广场开展以“关爱生命,关注消防”为主题的消防宣传片放映活动。消防志愿者服
以“创新·跨越”为主题的2012北京国际车展于2012年4月23日至5月2日以全新的境界和面貌在北京中国国际展览中心举行。汽车电子领域的领军品牌——卡仕达,以“声控更安全”为
胜利油田滩海地面工程,结合自己的实际和特权,坚持“安全、简便、经济、可靠、注重环保”由原则,自1993年至今陆续设计、建造、投产了冷组及单井采油平台ZO余座,中心平台1座(中已
雅俗论是中国美学的重要范畴。应用写作的文章风格和语言表达的基本要求是充实、准确、简洁和生动,但有时也要追求典雅,因为典雅是一种特殊的美。“典雅”的内涵极为丰富,和
总结了1985年1月~1994年12月间我科收治的27例青少年腰椎间盘突出症患者,并以信访疗效。认为:外伤是青少年腰椎间盘突出症的主要原因;先天性脊柱异常并非本病的决定因素;应重视临床体征,尤其是直