Synthesis Structure and Behavbr of Polymeric Drugs Covalently Linked 5 - Fluorouracil

来源 :Chemical Journal of Chinese Universities | 被引量 : 0次 | 上传用户:a490093469
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Four series of polymeric drugs with 5-Fluorouracil(5-FU) cova-lently linked in side chain were synthesized by the use of starch and carboxylmethylcellulose and two new 5-FU derivatives were also synthesized by using molecular sieve as a catalyst.Their structures were determined by IR,1H NMR and mass spectra.The changes in the Nitrogen content of polymeric drugs with reaction conditions and the influences of the N content on their limiting viscosity were studied.The hydrolysis of 5-FU from starch and carboxylmethylcellulose derivatives in various of buffer were researched by simulating physiologically acid-alkali enviroment.In addition,anticancer activity(in vivo and in vitro) of some starch derivative has been preliminaryly observed. Four series of polymeric drugs with 5-Fluorouracil (5-FU) cova-lently linked in side chain were synthesized by the use of starch and carboxylmethylcellulose and two new 5-FU derivatives were also synthesized by using molecular sieve as a catalyst.Their structures were determined by IR, 1H NMR and mass spectra. The changes in the Nitrogen content of polymeric drugs with reaction conditions and the influences of the N content on their limiting viscosity were studied. The hydrolysis of 5-FU from starch and carboxylmethylcellulose derivatives in various of buffer were researched by simulating physiologically acid-alkali enviroment. addition, anticancer activity (in vivo and in vitro) of some starch derivative has been initially observed.
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