Synthesis and Crystal Structure of 3-Benzyl-6-trichloromethyl- [ 1,2,4] triazolo[3,4-b][1,3,4]thiad

• 作 者: 张晶 雷新响 张力学 周长凤 付小旦
• 机 构: CollegeofChemistryandMaterialsScience
• 出 处: 结构化学
• 发表日期: 2009年8期
• 关键词: 晶体结构 核磁共振 X射线衍射 三氯甲基 元素分析 红外光谱 三斜晶系 相互作用 synthesis [1 2 4]triazolo[3 4-b][1 3 4
• 基金项目: This work was supported by the Natural Science Foundation of Zhejiang Province （No. M203149）

The title compound 3-benzyl-6-trichloromethyl-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole I (C11H7Cl3N4S,Mr = 333.62) has been synthesized,and its structure was determined by elemental analyses,IR,1H NMR,13C NMR,and X-ray diffractions. The crystal is of tric